首页 杂志概况 投稿须知 在线投稿 在线阅读 征订启事 广告服务 行业资讯 企业动态 资料中心  专访报道 会展信息 ENGLISH

引用本文:   何媛, 黄扬明, 王瑶, 赵悦婷, 李小斌, 张凤侠, 徐磊, 彭军仓, 闵顺耕. 近红外光谱和气相色谱-质谱联用分析烟用爆珠的研究. 分析化学, 2020, 48(9): 1244-1251. doi:  10.19756/j.issn.0253-3820.201140 [复制]

Citation:   HE Yuan , HUANG Yang-Ming , WANG Yao , ZHAO Yue-Ting , LI Xiao-Bin , ZHANG Feng-Xia , XU Lei , PENG Jun-Cang , MIN Shun-Geng . Analysis of Breakable Capsules for Cigarette Filter by Near-Infrared Spectroscopy and Gas Chromatography-Mass Spectrometry. Chinese Journal of Analytical Chemistry, 2020, 48(9): 1244-1251. doi: 10.19756/j.issn.0253-3820.201140 [复制]

近红外光谱和气相色谱-质谱联用分析烟用爆珠的研究

通讯作者:  彭军仓, pjc126@sina.com; 闵顺耕, minsg@263.com

收稿日期: 2020-03-18

基金项目: 本文系陕西中烟工业有限责任公司科技项目(No.ZB16020)资助

Analysis of Breakable Capsules for Cigarette Filter by Near-Infrared Spectroscopy and Gas Chromatography-Mass Spectrometry

Corresponding author:  PENG Jun-Cang , pjc126@sina.com; MIN Shun-Geng , minsg@263.com

Received Date:  2020-03-18

Fund Project:  This work was supported by the Science Foundation of China Tobacco Shaanxi Industrial Co. Ltd. (No. ZB16020).

分别采用近红外光谱(NIRS)和气相色谱-质谱联用(GC-MS)法分析了3种不同类型烟用爆珠。收集了清甜型、蜜甜型和薄荷型3种类型烟用爆珠的不同批次共27个样品,采集其NIRS谱图,通过光谱数据分析结合簇类独立软模式法(Soft independent modeling of class analogy,SIMCA)对3种烟用爆珠样品建立了分类模型,采用线性判别分析法(Linear discriminant analysis,LDA)对同一类型不同批次的烟用爆珠进行质量一致性评价,同时采用GC-MS法对3种类型烟用爆珠内含物中挥发性及半挥发性成分进行了分析。结果表明,烟用爆珠香型不同,其内含物挥发性及半挥发性成分差别较大;NIRS技术可以有效判别不同颜色壁材的爆珠;建立的SIMCA模型可区分3种类型烟用爆珠,且清甜型、蜜甜型和薄荷型烟用爆珠不同批次样品的区分准确度均在90%以上,建立的LDA模型可很好地区分3种类型不同批次的烟用爆珠。

关键词:   近红外光谱法, 气相色谱-质谱联用法, 烟用爆珠, 簇类独立软模式法, 线性判别分析法
Key words:   Near-infrared spectroscopy, Gas chromatography-mass spectrometry, Breakable capsule for cigarette filter, Soft independent modeling of class analogy, Linear discriminant analysis
[1]

Abad-Vivero E N, Thrasher J F, Arillo-Santillán E, Pérez-Hernández R, Barrientos-Gutíerrez I, Kollath-Cattano C, Mejía R, Sargent J D. Tob. Control,2016,25(E2):E113-E119

[2]

Thrasher J F, Abad-Vivero E N, Moodie C, O'Connor R J, Hammond D, Cummings K M, Yong H H, Salloum R G, Czoli C, Reynales-Shigematsu L M. Tob. Control,2016,25(3):275-283

[3]

Thrasher J F, Islam F, Barnoya J, Mejia R, Valenzuela M T, Chaloupka F J. Tob. Control,2017,26(4):468-470

[4]

Kim H S, Pack E C, Koo Y J, Lee Y J, Sung D K, Lee S H, Kim Y S, Kwon K H, Lim K M, Jang D Y, Choi D W. Regul. Toxicol. Pharm,2018,92:420-428

[5]

Jan U P, Dietmar R K, Reinhold C. Trends Food Sci. Tech. ,2015,46:211-230

[6]

Ebrahiema A, Olaniyi A F, Lembe S M, Umezuruike L O. J. Food Eng.,2018,217:11-23

[7]

Su W H, He H J, Sun D W. Crit. Rev. Food Sci. Nutri.,2017,57(5):1039-1051

[8]

Celio P. Anal. Chim. Acta,2018,1026:8-36

[9]

Mees C, Souard F, Delporte C, Deconinck E, Stoffelen P, Stévigny C, Kauffmann J M, Braekeleer K. Talanta,2018,177(15):4-11

[10]

BonaM T, Andrés J M. Talanta,2007,72(4):1423-1431

[11]

Jones R W, Reinot T, Frei U K, Tseng Y, Lubberstedt T, Mcclelland J F. Appl. Spectrosc.,2012,66(4):447-450

[12]

Okubo N, Kurata Y. Foods,2019,8(82):1-7

[13]

Liu L, Cozzolino D, Cynkar W U, Gishen M, Colby C B. J. Agric. Food Chem.,2006,54(18):6754-6759

[14]

Zhang Y, Cong Q, Xie Y, Yang J, Zhao B. Spectrochim. Acta A,2008, 71(4):1408-1413

[15]

Jing M, Cai W, Shao X. Anal. Lett.,2010,43(12):1910-1921

[16]

Bi Y, Yuan K, Xiao W, Wu J, Shi C, Xia J, Chu G, Zhang G, Zhou G. Anal. Chim. Acta,2016,909:30-40

[17]

Lobato K B S, Alamar P D, Caramês E T S, Pallone J A L. J. Food Eng.,2018,224:105-111

计量
  • PDF下载量(5)
  • 文章访问量(148)
  • HTML全文浏览量(4)

目录

近红外光谱和气相色谱-质谱联用分析烟用爆珠的研究

何媛, 黄扬明, 王瑶, 赵悦婷, 李小斌, 张凤侠, 徐磊, 彭军仓, 闵顺耕

Figures and Tables